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| Data is from Example 7.5 on page 347 in the book ''Response Surface Methodology, process and product optimization using design experiments, second edition,'' by Raymond H. Myers and Douglas C. Montgomery, John Wiley & Sons, Inc. 2002. | | Data is from Example 7.5 on page 347 in the book ''Response Surface Methodology: Process and Product Optimization Using Designed Experiments, 2nd Edition,'' by Raymond H. Myers and Douglas C. Montgomery, John Wiley & Sons, Inc. 2002. |
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This example validates the calculation of the Box-Behnken RSM method in DOE++.
Reference Case
Data is from Example 7.5 on page 347 in the book Response Surface Methodology: Process and Product Optimization Using Designed Experiments, 2nd Edition, by Raymond H. Myers and Douglas C. Montgomery, John Wiley & Sons, Inc. 2002.
Data
| Level (coded value)
|
Temperature (A)
|
Agitation (B)
|
Rate (C)
|
| High (+1) |
200 |
10 |
25
|
| Center (0) |
175 |
7.5 |
20
|
| Low (-1) |
150 |
5 |
15
|
The viscosity of the resin was recorded as an indirect measure of molecular weight.
| Standard order
|
A
|
B
|
C
|
Y
|
| 1 |
-1 |
-1 |
0 |
53
|
| 2 |
+1 |
-1 |
0 |
58
|
| 3 |
-1 |
+1 |
0 |
59
|
| 4 |
+1 |
+1 |
0 |
56
|
| 5 |
-1 |
0 |
-1 |
64
|
| 6 |
+1 |
0 |
-1 |
45
|
| 7 |
-1 |
0 |
+1 |
35
|
| 8 |
+1 |
0 |
+1 |
60
|
| 9 |
0 |
-1 |
-1 |
59
|
| 10 |
0 |
+1 |
-1 |
64
|
| 11 |
0 |
-1 |
+1 |
53
|
| 12 |
0 |
+1 |
+1 |
65
|
| 13 |
0 |
0 |
0 |
65
|
| 14 |
0 |
0 |
0 |
59
|
| 15 |
0 |
0 |
0 |
62
|
Result
From the book, the ANOVA table (partial sum of squares) is:
| Source
|
Partial SS
|
DF
|
Mean Square
|
F value
|
Prob>F
|
| Model |
882.48 |
9 |
98.05 |
9.57 |
0.0114
|
| A |
8 |
1 |
8.00 |
0.78 |
0.4174
|
| B |
55.12 |
1 |
55.12 |
5.38 |
0.0681
|
| C |
45.13 |
1 |
45.13 |
4.40 |
0.09
|
| [math]\displaystyle{ A^2 }[/math] |
200.83 |
1 |
200.83 |
19.59 |
0.0069
|
| [math]\displaystyle{ B^2 }[/math] |
12.98 |
1 |
12.98 |
1.27 |
0.3115
|
| [math]\displaystyle{ C^2 }[/math] |
48.52 |
1 |
48.52 |
4.73 |
0.0816
|
| AB |
16.00 |
1 |
16.00 |
1.56 |
0.2668
|
| AC |
484.00 |
1 |
484.00 |
47.22 |
0.001
|
| BC |
12.25 |
1 |
12.25 |
1.22 |
0.3241
|
| Residual |
51.25 |
5 |
10.25 |
|
|
| Lack of Fit |
33.25 |
3 |
11.08 |
1.23 |
0.4774
|
| Pure error |
18 |
2 |
9.00 |
|
|
| Cor total |
933.73 |
14 |
|
|
|
The final equation in terms of actual factors:
- [math]\displaystyle{ \begin{align}
Viscosity=-58.875+2.65 * Temp-0.65 * Agitation-11.125*Rate-0.0118*Temp^2+0.3*Agitation^2 \\
-0.145*Rate^2-0.032*Temp*Agitation+0.088*Temp*Rate+0.14*Agitation*Rate
\end{align} }[/math]
Results in DOE++
The software results match the book results. The ANOVA table is:
The final equation in terms of actual factors is:
